Diphenylacetic Acid → 5-{N'-(diphenylacetyl)-L-alaninyl}-amino-7-methyl-5,7-dihydro-6H-dibenz[b,d]azepin-6-one
反応式
[C:1]1([CH:7]([C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)[C:8]([OH:10])=O)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[NH2:17][C@H:18]([C:20]([N:22]1[C:28](=[O:29])[CH:27]([CH3:30])[C:26]2[CH:31]=[CH:32][CH:33]=[CH:34][C:25]=2[C:24]2[C:35]([NH2:39])=[CH:36][CH:37]=[CH:38][C:23]1=2)=[O:21])[CH3:19]>>[C:11]1([CH:7]([C:1]2[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=2)[C:8]([NH:17][C@H:18]([C:20]([N:22]2[C:28](=[O:29])[CH:27]([CH3:30])[C:26]3[CH:31]=[CH:32][CH:33]=[CH:34][C:25]=3[C:24]3[C:35]([NH2:39])=[CH:36][CH:37]=[CH:38][C:23]2=3)=[O:21])[CH3:19])=[O:10])[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1参加物
3
実験手順
Following General Procedure C-P above using diphenylacetic acid and 5-(L-alaninyl)-amino-7-methyl-5,7-dihydro-6H-dibenz[b,d]azepin-6-one, as described in Example 7-B, the title compound was prepared. The molecular weight as determined by mass spectrometry (FD) was: 504 (M+H).
出典と根拠
- ORDレコード
- ord-8c9b90b80b2c49a08857ea461d0b06fa
- 出典データセット
- uspto-grants-2003_05