化工社化工社 化学情報印刷レポート · 研究参考用
Glycine, N-acetyl-N-phenyl- → 5-{N'-(N-acetyl-N-phenylglycinyl)-L-alaninyl}-amino-7-methyl-5,7-dihydro-6H-dibenz[b,d]azepin-6-one
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Glycine, N-acetyl-N-phenyl- | HCID 68483 | — |
| 反応物 | 5-(L-alaninyl)-amino-7-methyl-5,7-dihydro-6H-dibenz[b,d]azepin-6-one | HCID 69736335 | — |
| 生成物 | 5-{N'-(N-acetyl-N-phenylglycinyl)-L-alaninyl}-amino-7-methyl-5,7-dihydro-6H-dibenz[b,d]azepin-6-one | HCID 86592605 | — |
反応手順
Following one or more of the general procedures outlined above, using acetyl-N-phenylglycine and 5-(L-alaninyl)-amino-7-methyl-5,7-dihydro-6H-dibenz[b,d]azepin-6-one, as described in Example 7-B, the title compound was prepared. The molecular weight as determined by mass spectrometry (FD) was: 485 (M+H).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06569851B1 |
| 出典データセット | uspto-grants-2003_05 |
| ORD ID | ord-7e257ba982834a7eba47fb77cb67c498 |
| 出典メモ | uspto-grants-2003_05 |