1,3-Bis(isocyanatomethyl)benzene → Hexamethylene diisocyanate

HRID 414110

反応式

HRID 414110 の反応式
[CH:1]1[CH:6]=[C:5](CN=C=O)[CH:4]=[C:3]([CH2:11][N:12]=[C:13]=[O:14])C=1.C1(CN=C=O)C(C[N:22]=[C:23]=[O:24])=CC=CC=1>>[CH2:1]([N:22]=[C:23]=[O:24])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:11][N:12]=[C:13]=[O:14]

参加物

3

反応物 2

HCID 192621,3-Bis(isocyanatomethyl)benzeneHCID 3035160Bis(isocyanatomethyl)benzene

生成物 1

HCID 13192Hexamethylene diisocyanate

実験手順

The same isocyanuration reaction as in Example 1 was carried out except that 3,290 g of hexamethylene diisocyanate and 210 g of "Takenate 500" (xylylene diisocyanate produced by Takeda Chemical Industry Co., Ltd.) were used instead of 3,500 g of hexamethylene diisocyanate, and the amount of the isocyanuration catalyst used in Example 1 was changed to 4.7 g. There was obtained 4,219 g of the reaction mixture containing the deactivated catalyst.

後処理

  1. customThe same isocyanuration reaction as in Example 1

出典と根拠

ORDレコード
ord-4b447846255647969ae905571ab14d0c
出典データセット
uspto-grants-1988_12
特許番号
US04789705

関連ノート

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