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HRID 414395作成日:2026年10月27日

2,6-Dimethylnaphthalene → 2,7-Dimethylnaphthalene

https://huagongshe.com/reaction/414395

反応式

関与物質

役割名称HCID仕込み量
反応物2,6-DimethylnaphthaleneHCID 11387—
反応物2,7-DimethylnaphthaleneHCID 11396—
溶媒P-XyleneHCID 7809—
生成物2,7-DimethylnaphthaleneHCID 11396—
生成物2,6-Dmn 2,7-dmnHCID 131715796—

反応手順

An agitation vessel of the same type as used in the crystallizing steps of Example 1 was charged with 152.2 g of a solution consisting of 2,6-DMN, 2,7-DMN and paraxylene at a weight ratio of 9:9:82 and the charged solution was cooled from 19.5° C. to 7.0° C. over a period of 72 minutes. The change in the composition of the liquid phase in the solution with time was analyzed and it was found that 2,6 -DMN and 2,7-DMN formed a eutectic mixture at a 2,6-DMN/2,7-DMN ratio of 0.59.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04791235
出典データセットuspto-grants-1988_12
ORD IDord-861ee37f3c3744f68d5e2072ebea0271
出典メモuspto-grants-1988_12