Calcium Carbonate → HCID 178419798、化合物

HRID 414628ノート

反応式

HRID 414628 の反応式
[S:1].[CH2:2]1[CH:6]2[C@@H:7]3[CH:11]=[CH:10][C@H:9]([CH:5]2[CH:4]=[CH:3]1)[CH2:8]3.C(=O)([O-])[O-].[Ca+2]>O>[S:1].[CH2:2]1[CH:6]2[C@@H:7]3[CH:11]=[CH:10][C@H:9]([CH:5]2[CH:4]=[CH:3]1)[CH2:8]3

参加物

5

反応物 3

HCID 10112Calcium CarbonateHCID 5362487SulfurHCID 15618652endo-Dicyclopentadiene

生成物 1

HCID 178419798HCID 178419798、化合物

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

Into a 4 liter autoclave were placed 425 g of sulfur, 75 g of DCPD, 2500 ml of water, 20 g of calcium carbonate and 5.0 g of Igepal®-630 (GAF). The reactor was sealed and heated to 150° for three hours with stirring. After cooling to room temperature, the sulfur/DCPD adduct was isolated as small ribbons.

後処理

  1. customThe reactor was sealed
  2. temperatureheated to 150° for three hours

出典と根拠

ORDレコード
ord-511ec55e90004ba1bae3a0571b85130c
出典データセット
uspto-grants-1988_12
特許番号
US04792589

反応ノート

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