関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Calcium Carbonate | HCID 10112 | — |
| 反応物 | Sulfur | HCID 5362487 | — |
| 反応物 | endo-Dicyclopentadiene | HCID 15618652 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | HCID 178419798 | HCID 178419798 | — |
反応手順
Into a 4 liter autoclave were placed 425 g of sulfur, 75 g of DCPD, 2500 ml of water and 20 g of calcium carbonate. The reactor was then sealed and heated to 150° C. for three hours with stirring. After cooling to ambient temperature, the sulfur/DCPD adduct was isolated as small beads.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04792589 |
|---|
| 出典データセット | uspto-grants-1988_12 |
|---|
| ORD ID | ord-0005c5c1607a4f3f973b1472511c893f |
|---|
| 出典メモ | uspto-grants-1988_12 |
|---|
