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Nitric Acid → 4-Methyl-6-nitro-7-hydroxy-1-indanone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Nitric Acid | HCID 944 | — |
| 反応物 | Acetic Anhydride | HCID 7918 | — |
| 反応物 | 7-Hydroxy-4-methyl-1-indanone | HCID 12436244 | — |
| 溶媒 | Acetic Acid | HCID 176 | — |
| 生成物 | 4-Methyl-6-nitro-7-hydroxy-1-indanone | HCID 13604142 | — |
反応手順
Into a solution of 25.6 g of 4-methyl-7-hydroxy-1-indanone in 250 ml of acetic acid was added 19.4 ml of acetic anhydride and a solution of 15.4 ml of concentrated nitric acid in 50 ml of acetic acid gradually. The reaction mixture was concentrated to drynsss, and the residue was washed with ether to obtain 25.7 g of 4-methyl-6-nitro-7-hydroxy-1-indanone.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04792628 |
| 出典データセット | uspto-grants-1988_12 |
| ORD ID | ord-5cb9e452ae114983b72b93924d0f9940 |
| 出典メモ | uspto-grants-1988_12 |