Carbon Dioxide → HCID 178527662、化合物

HRID 414882ノート

反応式

HRID 414882 の反応式
C(=O)([O-])[O-].[Ag+2:5].[CH2:6]([S:11]([OH:14])(=[O:13])=[O:12])[S:7]([OH:10])(=[O:9])=[O:8].C(=O)=O>O>[CH2:6]([S:11]([O-:14])(=[O:13])=[O:12])[S:7]([O-:10])(=[O:9])=[O:8].[Ag+2:5]

参加物

5

反応物 3

HCID 280Carbon DioxideHCID 10427Methanedisulfonic acidHCID 178418647HCID 178418647、化合物2 回

生成物 1

HCID 178527662HCID 178527662、化合物収率 123.7%

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

Silver carbonate (20 g, 0.0725 moles) was added to methanedisulfonic acid (25.55 g 50% solution in water) and diluted in 25 mL of distilled water while stirring. The silver carbonate dissolved with effervescence of carbon dioxide. After the reaction was complete, any remaining insoluble material was removed by filtration and the filtrate was stripped of water was removed under vacuum to give 25.3 g of pure silver methanedisulfonate.

後処理

  1. customany remaining insoluble material was removed by filtration
  2. customwas removed under vacuum

出典と根拠

ORDレコード
ord-7e11e4253b7d44f2a2c4ac9c3e72ef63
出典データセット
uspto-grants-2012_01
特許番号
US08088548B2

反応ノート

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