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HRID 41499作成日:2026年10月25日

Hydrogen Bromide → HCID 68820841、化合物

https://huagongshe.com/reaction/41499

反応式

関与物質

役割名称HCID仕込み量
反応物Hydrogen BromideHCID 260—
反応物Dimethyl SulfoxideHCID 679—
反応物methyl N-[3-(6,7-dimethoxy-2-methylaminoquinazolin-4-yl)phenyl]terephthalamic acidHCID 66646296—
溶媒IsopropanolHCID 3776—
生成物HCID 68820841HCID 68820841—

反応手順

Dimethyl sulfoxide (1 mL) and hydrobromic acid (40 μL) were added to methyl N-[3-(6,7-dimethoxy-2-methylaminoquinazolin-4-yl)phenyl]terephthalamic acid (100.90 mg). 2-Propanol (5 mL) was added to the mixture while heating the mixture, and the mixture was cooled to room temperature to be solidified. The solid was collected by filtration to yield the titled compound (108.92 mg).

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US08530654B2
出典データセットuspto-grants-2013_09
ORD IDord-c3aa049b7aa9465693f6054ed6d6261f
出典メモuspto-grants-2013_09