Hydrochloric Acid → 1,3,5-Tris-(p-(oct-1-yloxycarbonyl)-anilino)-s-triazine

HRID 4157

反応式

HRID 4157 の反応式
[NH2:1][C:2]1[CH:18]=[CH:17][C:5]([C:6]([O:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16])=[O:7])=[CH:4][CH:3]=1.[N:19]1[C:26](Cl)=[N:25][C:23](Cl)=[N:22][C:20]=1Cl.Cl>C1(C)C(C)=CC=CC=1>[CH2:9]([O:8][C:6]([C:5]1[CH:4]=[CH:3][C:2]([NH:1][N:19]2[CH2:26][N:25]([NH:1][C:2]3[CH:18]=[CH:17][C:5]([C:6]([O:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16])=[O:7])=[CH:4][CH:3]=3)[CH2:23][N:22]([NH:1][C:2]3[CH:3]=[CH:4][C:5]([C:6]([O:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16])=[O:7])=[CH:17][CH:18]=3)[CH2:20]2)=[CH:18][CH:17]=1)=[O:7])[CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]

参加物

5

反応物 3

HCID 313Hydrochloric AcidHCID 7954Cyanuric chlorideHCID 26629Octyl p-aminobenzoate

生成物 1

HCID 201527331,3,5-Tris-(p-(oct-1-yloxycarbonyl)-anilino)-s-triazine

試薬・触媒・溶媒 1

HCID 7237O-Xylene溶媒

反応条件

温度
90 °C

実験手順

75 g of octyl p-aminobenzoate and 18.5 g of cyanuric chloride in 1,000 ml of xylene were heated at 140° C. for 8 hours. After the evolution of hydrogen chloride was complete, the reaction solution was cooled to 90° C., washed twice with saturated sodium bicarbonate solution and once with water and then cooled to room temperature. The white crystals precipitated were filtered off under suction.

後処理

  1. washwashed twice with saturated sodium bicarbonate solution and once with water
  2. temperaturecooled to room temperature
  3. customThe white crystals precipitated
  4. filtrationwere filtered off under suction

出典と根拠

ORDレコード
ord-848069fa4f1f477c85839d23e4203cc5
出典データセット
uspto-grants-1988_02
特許番号
US04724137

関連ノート

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