関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | Cyanuric chloride | HCID 7954 | — |
| 反応物 | Decyl 4-aminobenzoate | HCID 4446056 | — |
| 溶媒 | O-Xylene | HCID 7237 | — |
| 生成物 | 1,3,5-Tris-(p-(dec-1-yloxycarbonyl)-anilino)-s-triazine | HCID 20152734 | — |
反応手順
83 g of decyl p-aminobenzoate and 18.5 g of cyanuric chloride in 1,000 ml of xylene were heated at 140° C. for 8 hours. After the evolution of hydrogen chloride was complete, the reaction solution was cooled to 90° C., washed twice with saturated sodium bicarbonate solution and once with water, and then cooled to room temperature. The white crystals precipitated were filtered off under suction and dried.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04724137 |
|---|
| 出典データセット | uspto-grants-1988_02 |
|---|
| ORD ID | ord-d7ec7c5243894addb439002cd6f1f99a |
|---|
| 出典メモ | uspto-grants-1988_02 |
|---|
