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2,3-Dichloro-4-hydroxybenzaldehyde → 1-(5-(4-Bromophenyl)thien-2-yl)-3-(2,3-dichloro-4-hydroxyphenyl)prop-2-en-1-one
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2,3-Dichloro-4-hydroxybenzaldehyde | HCID 528380 | — |
| 反応物 | 1-[5-(4-Bromophenyl)thiophen-2-yl]ethan-1-one | HCID 4231783 | — |
| 生成物 | 1-(5-(4-Bromophenyl)thien-2-yl)-3-(2,3-dichloro-4-hydroxyphenyl)prop-2-en-1-one | HCID 66624239 | — |
反応手順
1-(5-(4-Bromophenyl)thien-2-yl)-3-(2,3-dichloro-4-hydroxyphenyl)prop-2-en-1-one is prepared from 1-(5-(4-bromophenyl)thien-2-yl)ethanone and 2,3-dichloro-4-hydroxybenzaldehyde according to general procedure B. The evaporation residue is washed with dichloromethane.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08088819B2 |
| 出典データセット | uspto-grants-2012_01 |
| ORD ID | ord-99ab30ca15c64a4196374ccdb51f0af3 |
| 出典メモ | uspto-grants-2012_01 |