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Methyl iodide → 3-Hydroxy-2-iodo-1,6-dimethylpyridinium iodide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methyl iodide | HCID 6328 | — |
| 反応物 | 2-Iodo-6-methylpyridin-3-ol | HCID 89957 | — |
| 生成物 | 3-Hydroxy-2-iodo-1,6-dimethylpyridinium iodide | HCID 22266466 | — |
反応手順
2-Iodo-3-hydroxy-6-methylpyridine (835 mg) and iodomethane (3 mL) were added in glass sealed cube, and the reaction mixture was reacted at 130° C. for 4 h and at 180° C. for 1 h. The reaction mixture was completely evaporated to give 3-hydroxy-2-iodo-1,6-dimethylpyridinium iodide (2-014-02) (1.42 g).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08088924B2 |
| 出典データセット | uspto-grants-2012_01 |
| ORD ID | ord-ac5bfb723490414b8bfa5d7705e7c0c2 |
| 出典メモ | uspto-grants-2012_01 |