HCID 22266530、化合物 → 1-butyl-3-hydroxy-4(N,N-dimethylaminomethyl)pyridine-2-thione
反応式
[CH2:1]([N:5]1[CH:10]=[CH:9][CH:8]=[C:7]([OH:11])[C:6]1=[S:12])[CH2:2][CH2:3][CH3:4]>C(O)C>[CH2:1]([N:5]1[CH:10]=[CH:9][C:8]([CH2:1][N:5]([CH3:10])[CH3:6])=[C:7]([OH:11])[C:6]1=[S:12])[CH2:2][CH2:3][CH3:4]参加物
3
反応条件
- 温度
- 75 °C
実験手順
To a solution of 1-butyl-3-hydroxypyridine-2-thione (2-034-04) (1.0 g) in ethanol containing 10% water (20 mL) was added N, N, N′, N′-teteramethyldiaminomethane (1.70 g) at room temperature. After the reaction mixture was stirred at 75° C. for 24 h, the solvent was evaporated under reduced pressure to give 1-butyl-3-hydroxy-4(N,N-dimethylaminomethyl)pyridine-2-thione (2-034-05) (1.3 g, 95%) as an oil.
後処理
- customthe solvent was evaporated under reduced pressure
出典と根拠
- ORDレコード
- ord-d192df92636240e1a22cd6a213a9c0d9
- 出典データセット
- uspto-grants-2012_01
- 特許番号
- US08088924B2
反応ノート
読み込み中…