反応式
[NH:1]1[C:5]2[CH:6]=[CH:7][C:8]([NH2:10])=[CH:9][C:4]=2[N:3]=[CH:2]1.[S:11]1[CH2:16][CH2:15][N:14]([C:17]2[CH:24]=[CH:23][C:20]([CH:21]=O)=[CH:19][CH:18]=2)[CH2:13][CH2:12]1.C([O:27][C:28]([CH2:30][C:31](O)=[O:32])=O)C.C(=O)(OC)OC(C)(C)C[N+]#[C-].CC(C)([O-])C.[Na+]>>[NH:1]1[C:5]2[CH:6]=[CH:7][C:8]([N:10]3[CH:21]([C:20]4[CH:23]=[CH:24][C:17]([N:14]5[CH2:15][CH2:16][S:11][CH2:12][CH2:13]5)=[CH:18][CH:19]=4)[C:28](=[O:27])[CH2:30][C:31]3=[O:32])=[CH:9][C:4]=2[N:3]=[CH:2]1参加物
6
実験手順
The compound was synthesized starting from 1H-benzo[d]imidazol-5-amine (0.963 g, 7.24 mmol), 4-thiomorpholinobenzaldehyde (1.5 g, 7.24 mmol), 2-(ethoxycarbonyl)acetic acid (0.957 g, 7.24 mmol), 1-isocyano-2-methylpropan-2-yl methyl carbonate (1.13 g, 7.24 mmol) and sodium tert.-butoxide (0.77 g, 6.87 mmol) according to method 3.
後処理
- customThe compound was synthesized
出典と根拠
- ORDレコード
- ord-225648086b724bd2b3dbff6a448ccb30
- 出典データセット
- uspto-grants-2013_09
- 特許番号
- US08530670B2
関連ノート
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