化工社化工社 化学情報印刷レポート · 研究参考用
Diethylenetriaminepentaacetic acid → DTPA dianhydride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Diethylenetriaminepentaacetic acid | HCID 3053 | — |
| 反応物 | Acetic Anhydride | HCID 7918 | — |
| 溶媒 | Pyridine | HCID 1049 | — |
| 生成物 | DTPA dianhydride | HCID 100825 | — |
反応手順
1.08 gram of DTPA (2.7 mmol), 2 mL acetic anhydride and 1.3 mL pyridine were stirred for 48 hours at 60° C. and then the reaction mixture was filtered at room temperature. The solid product washed to be free of pyridine with acetic anhydride and then with diethyl ether, and is dried.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08532742B2 |
| 出典データセット | uspto-grants-2013_09 |
| ORD ID | ord-c95a531273a7400eacd53b7c1e81426f |
| 出典メモ | uspto-grants-2013_09 |