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llms.txt · MCPガイドプライバシーポリシー · 利用規約 · サポートv1.8.0
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1,2-Dichloroethane → Formate

HRID 418327
ノート
印刷プレビュー

反応式

HRID 418327 の反応式
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:19]=[CH:20][C:21]=1[O:22][CH3:23])[C:6]([NH:8][CH2:9][C:10]1[CH:11]=[C:12]([CH:16]=[CH:17][CH:18]=1)[C:13]([OH:15])=[O:14])=[O:7].C(Cl)CCl.C1C=CC2N(O)N=NC=2C=1.CN1CCOCC1.[CH3:45][N:46]([CH2:48][C:49]1[CH:50]=[C:51]([NH2:55])[CH:52]=[CH:53][CH:54]=1)[CH3:47]>CN(C=O)C>[CH3:47][N:46]([CH2:48][C:49]1[CH:50]=[C:51]([NH:55][C:13]([C:12]2[CH:11]=[C:10]([CH:18]=[CH:17][CH:16]=2)[CH2:9][NH:8][C:6](=[O:7])[C:5]2[CH:19]=[CH:20][C:21]([O:22][CH3:23])=[C:3]([O:2][CH3:1])[CH:4]=2)=[O:15])[CH:52]=[CH:53][CH:54]=1)[CH3:45].[CH:13]([O-:15])=[O:14]
参加物実験手順後処理出典と根拠反応ノート

参加物

8

反応物 5

HCID 111,2-DichloroethaneHCID 79724-MethylmorpholineHCID 757711-HydroxybenzotriazoleHCID 992943-amino-N,N-dimethylbenzylamineHCID 448195433-[(3,4-Dimethoxy-benzoylamino)-methyl]-benzoic acid

生成物 2

HCID 283Formate収率 1,399.3%
HCID 25054030
N-[3-(3-dimethylaminomethyl-phenylcarbamoyl)-benzyl]-3,4-dimethoxy-benzamide

試薬・触媒・溶媒 1

HCID 6228Dimethylformamide溶媒2 回

実験手順

3-[(3,4-Dimethoxy-benzoylamino)-methyl]-benzoic acid (40 mg, 0.127 mmol), prepared as described in Example 8, was combined with EDC (38.3 mg, 0.2 mmol) and HOBt (24.3 mg, 0.18 mmol) in a reaction vial, and DMF (1 mL) was added followed by N-methylmorpholine (0.025 mL, 0.22 mmol). The resulting mixture was agitated for 1 h, then 3-dimethylaminomethyl-phenylamine (25.5 mg, 0.17 mmol) was added as a solution in DMF (0.5 mL), and the resulting mixture was agitated overnight. The product was purified directly by preparative HPLC using an acetonitrile/water/formic acid gradient providing the title compound as a formate salt (40 mg, 70% yield), MS analysis electrospray, 448 (M+H).

後処理

  1. additionwas added
  2. stirringthe resulting mixture was agitated overnight
  3. customThe product was purified directly by preparative HPLC

出典と根拠

ORDレコード
ord-78ba5dfa3fb841de96e969a04a7d9213
出典データセット
uspto-grants-2012_01
DOI
10.6084/m9.figshare.5104873.v1
特許番号
US08093266B2

反応ノート

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