2-Methoxyaniline → 1-(2-Methoxyphenylcarbamoyl)cyclopropanecarboxylic acid
反応式
[C:1]1([NH:7][C:8]([C:10]2([C:13]([OH:15])=[O:14])[CH2:12][CH2:11]2)=[O:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:16][O:17]C1C=CC=CC=1N>>[CH3:16][O:17][C:6]1[CH:5]=[CH:4][CH:3]=[CH:2][C:1]=1[NH:7][C:8]([C:10]1([C:13]([OH:15])=[O:14])[CH2:11][CH2:12]1)=[O:9]参加物
3
実験手順
Following the procedure described above for the synthesis of compound 161 (Scheme 45), but replacing aniline for 2-methoxyaniline, title compound 172 was obtained in 44% yield. M/S (m/z): 236.0 (M+H).
出典と根拠
- ORDレコード
- ord-15ab14e4b7e44732b59a7694cef05636
- 出典データセット
- uspto-grants-2012_01
- 特許番号
- US08093264B2
反応ノート
読み込み中…