関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Sulfuric Acid | HCID 1118 | — |
| 反応物 | 2-(2-Bromoethyl)naphthalene | HCID 228270 | — |
| 生成物 | 2-(2-Bromoethyl)naphthalenesulfonic acid | HCID 86612694 | — |
反応手順
2-(2-bromoethyl)naphthalene (120 g) was stirred in an ice bath while fuming sulfuric acid (50 g) was slowly added dropwise. After the dropwise addition, the mixture was stirred at 0° C. for 30 hours, whereby 2-(2-bromoethyl)naphthalenesulfonic acid and a plurality of isomers were obtained, and then separated and purified.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US08093342B2 |
|---|
| 出典データセット | uspto-grants-2012_01 |
|---|
| ORD ID | ord-ebce4216be1f4dd7b193824955a78eba |
|---|
| 出典メモ | uspto-grants-2012_01 |
|---|
