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4-Chloro-N-methoxy-N-methylbenzamide → HCID 57942543、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Chloro-N-methoxy-N-methylbenzamide | HCID 11275663 | — |
| 反応物 | N-(2-Bromo-5-chloro-pyridin-3-yl)-4-chloro-N-methoxvmethyl-3-trifluoromethyl-benzenesulfonamide | HCID 57942086 | — |
| 生成物 | HCID 57942543 | HCID 57942543 | — |
反応手順
The title compound was prepared by procedure analogous to that described in Example 29 using N-(2-bromo-5-chloro-pyridin-3-yl)-4-chloro-N-methoxymethyl-3-trifluoromethyl-benzenesulfonamide and 4-chloro-N-methoxy-N-methyl-benzamide 1H NMR (400 MHz, CDCl3) δ10.61 (s, 1H), 8.37 (m, 1H), 8.16 (m, 1H), 8.09 (m, 1H), 7.84 (m, 1H), 7.77-7.75 (m, 2H), 7.53 (m, 1H), 7.42-7.40 (m, 2H), 7.23 (m, 1H) MS: (M+H)/z=509.0.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08093247B2 |
| 出典データセット | uspto-grants-2012_01 |
| ORD ID | ord-39de2979ca3f4967b38db498465588bd |
| 出典メモ | uspto-grants-2012_01 |