Hydrochloric Acid → methyl 1H-tetrazol-1-ylacetate

HRID 419839ノート

反応式

HRID 419839 の反応式
[N:1]1([CH2:6][C:7]([OH:9])=[O:8])[CH:5]=[N:4][N:3]=[N:2]1.Cl.O1CCOC[CH2:12]1>CO>[N:1]1([CH2:6][C:7]([O:9][CH3:12])=[O:8])[CH:5]=[N:4][N:3]=[N:2]1

参加物

5

反応物 3

HCID 313Hydrochloric AcidHCID 312751,4-DioxaneHCID 5432071-Tetrazolylacetic acid

生成物 1

HCID 3153776methyl 1H-tetrazol-1-ylacetate

試薬・触媒・溶媒 1

HCID 887Methanol溶媒

実験手順

A mixture of tetrazol-1-yl acetic acid (5 g, 39 mmol) and 4M hydrochloric acid in dioxan (100 μL) in methanol (50 mL) was heated under reflux for 18 hours. The cooled mixture was evaporated under reduced pressure to provide the title compound.

後処理

  1. temperaturewas heated
  2. temperatureunder reflux for 18 hours
  3. customThe cooled mixture was evaporated under reduced pressure

出典と根拠

ORDレコード
ord-1f14cc65617e4ae1985a9137fda2cfc7
出典データセット
uspto-grants-2012_01
特許番号
US08093400B2

反応ノート

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