化工社化工社 化学情報印刷レポート · 研究参考用
(3-Methoxyphenyl)boronic acid → 2-(3-Methoxyphenyl)-3-methyl-5-nitropyridine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | (3-Methoxyphenyl)boronic acid | HCID 2734370 | — |
| 反応物 | 2-Bromo-3-methyl-5-nitropyridine | HCID 5200466 | — |
| 生成物 | 2-(3-Methoxyphenyl)-3-methyl-5-nitropyridine | HCID 67394162 | 72% |
反応手順
Obtained (2.43 g, yield 72%) following the procedure described in Intermediate 27, starting with 2-bromo-3-methyl-5-nitropyridine (13.82 mmol, 3.0 g), 3-methoxyphenylboronic acid (13.82 mmol, 2.10 g).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08536165B2 |
| 出典データセット | uspto-grants-2013_09 |
| ORD ID | ord-92a63ddccc2b42dfbab22f3eabf0d2ee |
| 出典メモ | uspto-grants-2013_09 |