化工社化工社 化学情報印刷レポート · 研究参考用
2-Bromo-5-iodo-3-methylpyridine → Ethyl 2-(6-bromo-5-methylpyridin-3-ylamino)-5-methylbenzoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Bromo-5-iodo-3-methylpyridine | HCID 10108680 | — |
| 反応物 | Ethyl 2-amino-5-methylbenzoate | HCID 12327280 | — |
| 生成物 | Ethyl 2-(6-bromo-5-methylpyridin-3-ylamino)-5-methylbenzoate | HCID 86657258 | 25% |
反応手順
Obtained (0.050 g, yield 25%) following the procedure described in Intermediate 16 starting with ethyl 2-amino-5-methylbenzoate (0.56 mmol, 0.100 g) and 2-bromo-5-iodo-3-methylpyridine (1.0 mmol, 0.166 g).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08536165B2 |
| 出典データセット | uspto-grants-2013_09 |
| ORD ID | ord-fd08ee6b90a440f8a547e6b85ab5b924 |
| 出典メモ | uspto-grants-2013_09 |