Benzenamine, 2-chloro-5-(trifluoromethyl)- → N-[2-Chloro-5-(trifluoromethyl)phenyl]-2-hydroxy-5-methoxybenzamide

HRID 421116

反応式

HRID 421116 の反応式
[CH3:1][O:2][C:3]1[CH:11]=[C:7]([C:8]([OH:10])=O)[C:6]([OH:12])=[CH:5][CH:4]=1.[Cl:13][C:14]1[CH:20]=[CH:19][C:18]([C:21]([F:24])([F:23])[F:22])=[CH:17][C:15]=1[NH2:16]>>[Cl:13][C:14]1[CH:20]=[CH:19][C:18]([C:21]([F:23])([F:24])[F:22])=[CH:17][C:15]=1[NH:16][C:8](=[O:10])[C:7]1[CH:11]=[C:3]([O:2][CH3:1])[CH:4]=[CH:5][C:6]=1[OH:12]

参加物

3

反応物 2

HCID 8475Benzenamine, 2-chloro-5-(trifluoromethyl)-HCID 757875-Methoxysalicylic Acid

生成物 1

HCID 17860112N-[2-Chloro-5-(trifluoromethyl)phenyl]-2-hydroxy-5-methoxybenzamide収率 56.4%

実験手順

Using 5-methoxysalicylic acid and 2-chloro-5-(trifluoromethyl)aniline as the raw materials, the same operation as the example 16 gave the title compound.

出典と根拠

ORDレコード
ord-b961c2af5a10453ba78d3f7fa5fddb3b
出典データセット
uspto-grants-2012_01
特許番号
US08097759B2

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