5-Chlorosalicylic Acid → 5-Chloro-2-hydroxy-N-(2,3,4,5,6-pentafluorophenyl)benzamide

HRID 421138

反応式

HRID 421138 の反応式

[Cl:1][C:2]1[CH:10]=[C:6]([C:7]([OH:9])=O)[C:5]([OH:11])=[CH:4][CH:3]=1.[F:12][C:13]1[C:19]([F:20])=[C:18]([F:21])[C:17]([F:22])=[C:16]([F:23])[C:14]=1[NH2:15]>>[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([OH:11])=[C:6]([CH:10]=1)[C:7]([NH:15][C:14]1[C:16]([F:23])=[C:17]([F:22])[C:18]([F:21])=[C:19]([F:20])[C:13]=1[F:12])=[O:9]

参加物

3

反応物 2

HCID 94475-Chlorosalicylic Acid

HCID 13040Pentafluoroaniline

生成物 1

HCID 178602165-Chloro-2-hydroxy-N-(2,3,4,5,6-pentafluorophenyl)benzamide収率 58.6%

実験手順

Using 5-chlorosalicylic acid and 2,3,4,5,6-pentafluoroaniline as the raw materials, the same operation as the example 16 gave the title compound.

出典と根拠

ORDレコード: ord-65d2cfb6d8224d47991fb0e281f69ec4
出典データセット: uspto-grants-2012_01
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US08097759B2

関連ノート

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