3,5-Di-tert-butylaniline → N-{3,5-Bis[(1,1-dimethyl)ethyl]phenyl}-2-hydroxy-5-methoxybenzamide

HRID 421153

反応式

HRID 421153 の反応式
[CH3:1][O:2][C:3]1[CH:11]=[C:7]([C:8]([OH:10])=O)[C:6]([OH:12])=[CH:5][CH:4]=1.[CH3:13][C:14]([C:17]1[CH:18]=[C:19]([CH:21]=[C:22]([C:24]([CH3:27])([CH3:26])[CH3:25])[CH:23]=1)[NH2:20])([CH3:16])[CH3:15]>>[CH3:16][C:14]([C:17]1[CH:18]=[C:19]([NH:20][C:8](=[O:10])[C:7]2[CH:11]=[C:3]([O:2][CH3:1])[CH:4]=[CH:5][C:6]=2[OH:12])[CH:21]=[C:22]([C:24]([CH3:27])([CH3:26])[CH3:25])[CH:23]=1)([CH3:13])[CH3:15]

参加物

3

反応物 2

HCID 754193,5-Di-tert-butylanilineHCID 757875-Methoxysalicylic Acid

生成物 1

HCID 66657198N-{3,5-Bis[(1,1-dimethyl)ethyl]phenyl}-2-hydroxy-5-methoxybenzamide収率 12.7%

実験手順

Using 5-methoxysalicylic acid and 3,5-bis[(1,1-dimethyl)ethyl]aniline as the raw materials, the same operation as the example 16 gave the title compound.

出典と根拠

ORDレコード
ord-b2c55289a3a143c6b8cc4321c379eb5f
出典データセット
uspto-grants-2012_01
特許番号
US08097759B2

関連ノート

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