2-Bromo-4-fluorobenzoic acid → 2-Bromo-4-fluoro-1-(methoxymethoxymethyl)benzene

反応式

[Br:1][C:2]1[CH:10]=[C:9]([F:11])[CH:8]=[CH:7][C:3]=1[C:4](O)=[O:5].BrC1C=CC(Cl)=CC=1[CH2:20][O:21][CH2:22]OC>>[Br:1][C:2]1[CH:10]=[C:9]([F:11])[CH:8]=[CH:7][C:3]=1[CH2:4][O:5][CH2:20][O:21][CH3:22]

参加物

反応物 2

HCID 12681692-Bromo-4-fluorobenzoic acid

HCID 590246772-Bromo-5-chloro-1-(methoxymethoxymethyl)benzene

生成物 1

HCID 667046952-Bromo-4-fluoro-1-(methoxymethoxymethyl)benzene

実験手順

This compound was made from 2-bromo-4-fluorobenzoic acid in the same manner as compound 18d and was used for the next step without purification.

後処理

customwas used for the next step without purification

出典と根拠

ORDレコード: ord-26cf496ab9514195b1fb5c9f9bcb4470
出典データセット: uspto-grants-2012_01
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US08106031B2

反応ノート

読み込み中…