反応式
[CH2:1]=[CH:2][S:3]([O-:6])(=[O:5])=[O:4].[Na+:7].[CH3:8][NH:9][CH3:10]>>[CH3:8][N:9]([CH3:10])[CH2:1][CH2:2][S:3]([O-:6])(=[O:5])=[O:4].[Na+:7]参加物
3
実験手順
Sodium ethylenesulfonate (18.2 ml, 25% aqueous solution w/w) and dimethylamine (4.43 ml, 40% aqueous solution w/w) were heated in a sealed finger tube at 105° C. for 48 h before concentrating in vacuo to yield the subtitle compound as a white solid. Yield: 9.80 g.
後処理
- concentrationbefore concentrating in vacuo
出典と根拠
- ORDレコード
- ord-3b9b1bfe3c984dff9ebaf9513b9644c9
- 出典データセット
- uspto-grants-2012_01
- 特許番号
- US08106063B2
関連ノート
読み込み中…