Acetic Anhydride → HCID 22403906、化合物

反応式

[NH2:1][C:2]1[CH:11]=[C:10]([C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)[C:9]2[C:4](=[CH:5][CH:6]=[C:7]([Cl:18])[CH:8]=2)[N:3]=1.[C:19](OC(=O)C)(=[O:21])[CH3:20]>>[C:19]([NH:1][C:2]1[CH:11]=[C:10]([C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)[C:9]2[C:4](=[CH:5][CH:6]=[C:7]([Cl:18])[CH:8]=2)[N:3]=1)(=[O:21])[CH3:20]

参加物

反応物 2

HCID 7918Acetic Anhydride

HCID 672273HCID 672273、化合物

生成物 1

HCID 22403906HCID 22403906、化合物

反応条件

温度: 70 °C

実験手順

A mixture of 0.1 g of 2-amino-6-chloro-4-phenylquinoline and 8 ml of acetic anhydride was stirred at 70° C. for 1 hour, the solvent was removed by distillation, the solid residue was stirred with water, and the crystalline substance was filtered off.

後処理

customthe solvent was removed by distillation
stirringthe solid residue was stirred with water
filtrationthe crystalline substance was filtered off

出典と根拠

ORDレコード: ord-cccb3e67d18d4380b9c159108951512a
出典データセット: uspto-grants-2012_01
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US08106204B2

反応ノート

読み込み中…

参加物