化工社化工社 化学情報印刷レポート · 研究参考用
Isonicotinic Acid → Isonicotinoyl chloride hydrochloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Isonicotinic Acid | HCID 5922 | — |
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 生成物 | Isonicotinoyl chloride hydrochloride | HCID 12262826 | — |
反応手順
A solution of isonicotinic acid (0.10 g, 0.8 mmol) and thionyl chloride (1 mL) were heated to reflux for 2 h and concentrated. The product obtained was used immediately in the following step.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08536194B2 |
| 出典データセット | uspto-grants-2013_09 |
| ORD ID | ord-0d0bda2a4ecf4b5fa1825fca2cb4ad7b |
| 出典メモ | uspto-grants-2013_09 |