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(2-Bromophenyl)boronic acid → 5-(2-Bromophenyl)-1,3-benzodioxole-4-carbaldehyde
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | (2-Bromophenyl)boronic acid | HCID 2773294 | — |
| 反応物 | 5-Bromo-1,3-benzodioxole-4-carboxaldehyde | HCID 11031640 | — |
| 生成物 | 5-(2-Bromophenyl)-1,3-benzodioxole-4-carbaldehyde | HCID 86658680 | — |
反応手順
The process described in Method B was followed. 5-Bromo-1,3-benzodioxole-4-carbaldehyde (1.15 g, 5.00 mmol) and 2-bromophenylboronic acid (1.10 g, 5.50 mmol) were used to obtain the title compound. The crude product was purified by column chromatography with a mixture of hexane:ethyl acetate (9:1) as the eluent.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08536210B2 |
| 出典データセット | uspto-grants-2013_09 |
| ORD ID | ord-89304411dabb487c91269d35b72d6f0f |
| 出典メモ | uspto-grants-2013_09 |