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Methanol → HCID 58484330、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methanol | HCID 887 | — |
| 反応物 | 6-Chloro-5-formyl-1,3-dimethyluracil | HCID 319971 | — |
| 生成物 | HCID 58484330 | HCID 58484330 | — |
反応手順
The process described in Method C was followed. 6-Chloro-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde (0.270 g, 1.33 mmol) and methanol were used to obtain the title compound. The crude product was purified by column chromatography with a mixture of n-hexane:ethyl acetate (4:1) as the eluent.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08536210B2 |
| 出典データセット | uspto-grants-2013_09 |
| ORD ID | ord-c85dff6070af47f89ad63f95a7464379 |
| 出典メモ | uspto-grants-2013_09 |