Potassium Carbonate → HCID 12698958、化合物

HRID 426950ノート

反応式

HRID 426950 の反応式
Cl.[CH:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH:5]=[CH:4][C:3]=1[CH:12]([O:19][CH3:20])[CH2:13][N:14]1[CH:18]=[CH:17][N:16]=[CH:15]1.C(=O)([O-])[O-].[K+].[K+]>ClCCl>[CH:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH:5]=[CH:4][C:3]=1[CH:12]([O:19][CH3:20])[CH2:13][N:14]1[CH:18]=[CH:17][N:16]=[CH:15]1

参加物

4

反応物 2

HCID 11430Potassium CarbonateHCID 126989591-[2-(2-Naphthyl)-2-(methoxy)ethyl]imidazole hydrochloride

生成物 1

HCID 12698958HCID 12698958、化合物

試薬・触媒・溶媒 1

HCID 6344Dichloromethane溶媒

実験手順

1-[2-(2-naphthyl)-2-(methoxy)ethyl]imidazole hydrochloride (800 mg.) in 50 ml. of dichloromethane is shaken with excess dilute potassium carbonate solution until the salt is completely neutralized. The organic layer is then separated, washed twice with water, dried over magnesium sulfate and evaporated to yield 1-[2-(2-naphthyl)-2-(methoxy)ethyl]-imidazole.

後処理

  1. customThe organic layer is then separated
  2. washwashed twice with water
  3. dry with materialdried over magnesium sulfate
  4. customevaporated

出典と根拠

ORDレコード
ord-99037d6b6ad94f718cce4b2a707f09d1
出典データセット
uspto-grants-1979_10
特許番号
US04172141

反応ノート

読み込み中…