化工社化工社 化学情報印刷レポート · 研究参考用
Ethanethiol → 6-(Ethylthio)-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethanethiol | HCID 6343 | — |
| 反応物 | 6-Chloro-5-formyl-1,3-dimethyluracil | HCID 319971 | — |
| 生成物 | 6-(Ethylthio)-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde | HCID 58484335 | — |
反応手順
The process described in Method D was followed. 6-Chloro-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde (0.303 g, 1.50 mmol) and ethanethiol were used to obtain the title compound. The crude product was purified by column chromatography with a mixture of n-hexane:ethyl acetate (1:1) as the eluent.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08536210B2 |
| 出典データセット | uspto-grants-2013_09 |
| ORD ID | ord-dbafb17038e6410e997a1aa39eb95162 |
| 出典メモ | uspto-grants-2013_09 |