反応式
Cl[C:2]1[N:7]([CH3:8])[C:6](=[O:9])[N:5]([CH3:10])[C:4](=[O:11])[C:3]=1[CH:12]=[O:13].[CH2:14]([SH:16])[CH3:15]>>[CH2:14]([S:16][C:2]1[N:7]([CH3:8])[C:6](=[O:9])[N:5]([CH3:10])[C:4](=[O:11])[C:3]=1[CH:12]=[O:13])[CH3:15]参加物
3
実験手順
The process described in Method D was followed. 6-Chloro-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde (0.303 g, 1.50 mmol) and ethanethiol were used to obtain the title compound. The crude product was purified by column chromatography with a mixture of n-hexane:ethyl acetate (1:1) as the eluent.
出典と根拠
- ORDレコード
- ord-dbafb17038e6410e997a1aa39eb95162
- 出典データセット
- uspto-grants-2013_09
- 特許番号
- US08536210B2
関連ノート
読み込み中…