化工社化工社 化学情報印刷レポート · 研究参考用
Benzyloxyamine hydrochloride → 6-(Ethylthio)-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde O-benzyloxime
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzyloxyamine hydrochloride | HCID 102312 | — |
| 反応物 | 6-(Ethylthio)-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde | HCID 58484335 | — |
| 生成物 | 6-(Ethylthio)-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde O-benzyloxime | HCID 86658688 | — |
反応手順
The process described in Method A was followed. 6-(Ethylthio)-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde (Example 23, Step 1) (0.070 mg, 0.30 mmol) and O-benzyl-hydroxylamine hydrochloride (0.063 mg, 0.40 mmol) were used to obtain the title compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08536210B2 |
| 出典データセット | uspto-grants-2013_09 |
| ORD ID | ord-e53f4ee389a449ed958feb11973d33af |
| 出典メモ | uspto-grants-2013_09 |