化工社化工社 化学情報印刷レポート · 研究参考用
Sodium Hydroxide → 4,4'-Bis(hydroxymethyl)biphenyl
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | 4,4'-Bis(acetoxymethyl)biphenyl | HCID 11335507 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | 4,4'-Bis(hydroxymethyl)biphenyl | HCID 611786 | 80% |
反応手順
0.1 moles 4,4'bis(acetoxymethyl)biphenyl (prepared by method C above), 0.4 mole sodium hydroxide as 23 percent aqueous solution and 50 mls ethanol were refluxed for 3 hours with stirring. The reaction mixture was filtered and the precipitate washed with water and dried to yield 0.08 moles product=80 percent of theory. m.p. 195°-97° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04172858 |
| 出典データセット | uspto-grants-1979_10 |
| ORD ID | ord-e0db6938a15b46bc973c1327f6ad7f43 |
| 出典メモ | uspto-grants-1979_10 |