関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | O-Methylhydroxylamine | HCID 4113 | — |
| 反応物 | 1-Acetylcyclohexene | HCID 13612 | — |
| 溶媒 | Acetic Acid | HCID 176 | — |
| 生成物 | cyclohexenyl-ethanone O-methyl-oxime | HCID 78148622 | — |
反応手順
To a stirred solution of a cyclohexenyl-ethanone (0.06 mmol), in acetic acid (500 μl) was added methoxyamine (4.7 mg). The reaction mixture was stirred at 24° C. for 48 h under nitrogen to obtain the cyclohexenyl-ethanone O-methyl-oxime.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US08536215B2 |
|---|
| 出典データセット | uspto-grants-2013_09 |
|---|
| ORD ID | ord-57036d9ef90e40e0a656d26d4659e650 |
|---|
| 出典メモ | uspto-grants-2013_09 |
|---|
