Acetic Anhydride → N-(2-(4-Benzoylphenylamino)phenyl)acetamide

HRID 428294ノート

反応式

HRID 428294 の反応式
[NH2:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[NH:8][C:9]1[CH:22]=[CH:21][C:12]([C:13]([C:15]2[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=2)=[O:14])=[CH:11][CH:10]=1.[C:23](OC(=O)C)(=[O:25])[CH3:24]>>[C:13]([C:12]1[CH:21]=[CH:22][C:9]([NH:8][C:3]2[CH:4]=[CH:5][CH:6]=[CH:7][C:2]=2[NH:1][C:23](=[O:25])[CH3:24])=[CH:10][CH:11]=1)(=[O:14])[C:15]1[CH:16]=[CH:17][CH:18]=[CH:19][CH:20]=1

参加物

3

反応物 2

HCID 7918Acetic AnhydrideHCID 11737779{4-[(2-Aminophenyl)amino]phenyl}(Phenyl)methanone2 回

生成物 1

HCID 18358189N-(2-(4-Benzoylphenylamino)phenyl)acetamide

実験手順

4-(2-Aminophenylamino)benzophenone (Compound 101, 0.58 g, 2 mmol) was dissolved in acetic anhydride (10 ml) and the solution was stirred at room temperature for 3 hours. The precipitate that forms after 75 min was filtered off and washed with water to afford the title compound.

後処理

  1. waitThe precipitate that forms after 75 min
  2. filtrationwas filtered off
  3. washwashed with water

出典と根拠

ORDレコード
ord-3626457397764f5681709ebfb618c5cb
出典データセット
uspto-grants-2001_11
特許番号
US06313174B1

反応ノート

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