化工社化工社 化学情報印刷レポート · 研究参考用
Hydrochloric Acid → (2,6-Dichlorophenyl)methanesulfonamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | Ammonium Hydroxide | HCID 14923 | — |
| 反応物 | (2,6-Dichlorophenyl)methanesulfonyl chloride | HCID 594465 | — |
| 生成物 | (2,6-Dichlorophenyl)methanesulfonamide | HCID 13631936 | 64% |
反応手順
The 2,6-dichlorobenzylsulfonylchloride (27 g, 103.6 mmol) in ammonium hydroxide (270 ml) was stirred at room temperature for 3 hours. On acidification with cooled concentrated hydrochloric acid a precipitate separated and was filtered to give desired product (16 g, 64%) MS(EI) m/e 239 (M−).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06316478B1 |
| 出典データセット | uspto-grants-2001_11 |
| ORD ID | ord-0cca67bc26fc480983a683f2d36302d8 |
| 出典メモ | uspto-grants-2001_11 |