関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Phthalic Anhydride | HCID 6811 | — |
| 反応物 | Hydroxylammonium phosphate (3:1) | HCID 10176537 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | N-Hydroxyphthalimide | HCID 10665 | — |
反応手順
1.48 g (10.0 mmol) of phthalic anhydride and 0.723 g (3.67 mmol) of hydroxylammonium phosphate were pulverized, mixed and, following the addition of 2 ml of water, heated at a bath temperature of 130° C. for about 1½ hours. The cooled lemon-yellow reaction mixture was diluted with water, and the solid was filtered off with suction, washed with water and dried at 50° C. The yield was 1.39 g (86%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US06316639B1 |
|---|
| 出典データセット | uspto-grants-2001_11 |
|---|
| ORD ID | ord-ffb4abcd931e499bb3815317beb34444 |
|---|
| 出典メモ | uspto-grants-2001_11 |
|---|
