関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Phthalic Anhydride | HCID 6811 | — |
| 反応物 | Hydroxylamine sulfate | HCID 24846 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | N-Hydroxyphthalimide | HCID 10665 | — |
反応手順
0.15 g (1.0 mmol) of phthalic anhydride was mixed with 0.2 to 1 equivalent of hydroxylammonium sulfate (see Table 1) and, optionally after the addition of water (see Table 1), heated to 130° C. in a sealed ampoule. The reaction times were varied for the individual mixtures in accordance with Table 1. The cooled reaction mixture was dissolved in d6-DMSO and analyzed using 1H-NMR spectroscopy. The yields are given in each case in Table 1.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US06316639B1 |
|---|
| 出典データセット | uspto-grants-2001_11 |
|---|
| ORD ID | ord-e3ee272c6b29480f9ca62db9970c86f7 |
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| 出典メモ | uspto-grants-2001_11 |
|---|
