Tetrafluoro-m-phenylenediamine dihydrochloride → 9,10-Anthracenedione, 1,4-bis((2-(dimethylamino)ethyl)amino)-5,8-dihydroxy-

反応式

C1(N)C(F)=C(F)C(F)=C(N)C=1F.Cl.Cl.[CH3:15][N+:16]([O-])([CH2:18][CH2:19][NH:20][C:21]1[CH:26]=[CH:25][C:24]([NH:27][CH2:28][CH2:29][N+:30]([O-])([CH3:32])[CH3:31])=[C:23]2[C:34]([C:36]3[C:41]([C:42](=[O:43])[C:22]=12)=[C:40]([OH:44])[CH:39]=[CH:38][C:37]=3[OH:45])=[O:35])[CH3:17]>>[CH3:31][N:30]([CH3:32])[CH2:29][CH2:28][NH:27][C:24]1[C:23]2[C:34](=[O:35])[C:36]3[C:41](=[C:40]([OH:44])[CH:39]=[CH:38][C:37]=3[OH:45])[C:42](=[O:43])[C:22]=2[C:21]([NH:20][CH2:19][CH2:18][N:16]([CH3:17])[CH3:15])=[CH:26][CH:25]=1

参加物

反応物 2

HCID 149026Tetrafluoro-m-phenylenediamine dihydrochloride2 回

HCID 9955116Banoxantrone

生成物 1

HCID 1354689,10-Anthracenedione, 1,4-bis((2-(dimethylamino)ethyl)amino)-5,8-dihydroxy-

実験手順

The solid dihydrochloride should be stored in a sealed container in a cold dark place (preferably a freezer). Before opening such containers they should be allowed to warm to room temperature, since the dihydrochloride (and AQ4N) absorb moisture particularly rapidly when cold.

後処理

customabsorb moisture particularly rapidly when cold

出典と根拠

ORDレコード: ord-48938090c62842d98ebb00d0f1203e2c
出典データセット: uspto-grants-2001_11
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US06320063B1

反応ノート

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