化工社化工社 化学情報印刷レポート · 研究参考用
Styrene → p-Tert-butoxystyrene styrene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Styrene | HCID 7501 | — |
| 反応物 | 1-(Tert-butoxy)-4-ethenylbenzene | HCID 577531 | — |
| 生成物 | p-Tert-butoxystyrene styrene | HCID 69102216 | — |
反応手順
With the use of 81.1 g (0.46 mole) of p-tert-butoxystyrene and 4.6 g (0.04 mole) of styrene, the same polymerization reaction and after-treatment as Production example 2-(1) were conducted to give 77.1 g of poly(p-tert-butoxystyrene/styrene) as white powders. A ratio of p-tert-butoxystyrene unit and styrene unit in the obtained polymer was about 92:8 by 1HNMR. Mw: about 20000, molecular dispersion: 1.90 (GPC method; polystyrene as standard).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06656660B1 |
| 出典データセット | uspto-grants-2003_12 |
| ORD ID | ord-b886aeadfd1d4c3f8ef665a00c2f0cf7 |
| 出典メモ | uspto-grants-2003_12 |