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Pyridine → 9-Anthracenylmethyl-1-piperazinecarboxylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Pyridine | HCID 1049 | — |
| 反応物 | Piperazine | HCID 4837 | — |
| 反応物 | 9-Anthracenemethanol | HCID 73848 | — |
| 反応物 | 4-Nitrophenyl chloroformate | HCID 82129 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | 9-Anthracenylmethyl-1-piperazinecarboxylate | HCID 9840073 | — |
反応手順
PAC is produced by adding 9-anthacenemethanol and pyridine to a solution of p-nitrophenyl chloroformate. Product is isolated to provide a crude anthrylmethyl p-nitrophenyl carbonate, which is then added to a solution of piperazine. The reacted mixture is poured into water and extracted with a solvent, preferably an organic solvent such as toluene. The product is washed and dried to provide 9-anthracenylmethyl-1-piperazinecarboxylate (PAC).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06656737B1 |
| 出典データセット | uspto-grants-2003_12 |
| ORD ID | ord-93be286c94a04903a525ad5c7e904ac7 |
| 出典メモ | uspto-grants-2003_12 |