化工社化工社 化学情報印刷レポート · 研究参考用
2-Aminothiazole → Cyclohexyl-[6-(2,4-dimethyl-phenyl)-imidazo[2,1-b]thiazol-5-yl]-amine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Aminothiazole | HCID 2155 | — |
| 反応物 | 2,4-Dimethylbenzaldehyde | HCID 61814 | — |
| 反応物 | Cyclohexyl isocyanide | HCID 79129 | — |
| 溶媒 | Perchloric Acid | HCID 24247 | — |
| 生成物 | Cyclohexyl-[6-(2,4-dimethyl-phenyl)-imidazo[2,1-b]thiazol-5-yl]-amine | HCID 22335581 | — |
反応手順
Compound 50 was prepared in accordance with the general synthesis instructions from 1.0 ml (0.1 mmol) 2-amino thiazole solution (0.1 M, MC), 0.575 ml (0.115 mmol) cyclohexylisonitrile solution (0.2 M, MC), 0.500 ml (0.15 mmol) 2,4-dimethylbenzaldehyde solution (0.3 M, MC) and 10 μl perchloric acid (w=20%) in a substance library.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06657064B2 |
| 出典データセット | uspto-grants-2003_12 |
| ORD ID | ord-2e0724f52e6d46bd9d1719219e1b4490 |
| 出典メモ | uspto-grants-2003_12 |