Methane → (2Z)-4-(Dodecylamino)-4-oxo-2-butenoic acid
反応式
[CH2:1]([NH:13][C:14](=[O:20])/[CH:15]=[CH:16]\[C:17]([OH:19])=[O:18])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].C(N)(=O)/C=C\C(O)=O.C>C1(C)C=CC=CC=1>[CH2:1]([NH:13][C:14](=[O:20])/[CH:15]=[CH:16]\[C:17]([OH:19])=[O:18])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]参加物
4
実験手順
2 g maleic acid amide N-dodecylmaleic acid amide are dissolved in 150 ml toluene and compounded with 10 g black (FW 1 or Printex Alpha). The suspension is boiled four hours under reflux and then drawn off, washed with acetone and dried eight hours in a drying oven at 105° C. The resulting black carries dodecyl groups.
後処理
- temperatureunder reflux
- washwashed with acetone
- customdried eight hours in a drying oven at 105° C
出典と根拠
- ORDレコード
- ord-bb99cb162650402781f747fda65ff5fd
- 出典データセット
- uspto-grants-2003_12
- 特許番号
- US06660075B2
反応ノート
読み込み中…