反応式
[C:1]([OH:12])(=[O:11])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9]C.[CH2:13]1CC[CH:16]([N:19]=[C:20]=[N:21][CH:22]2[CH2:27][CH2:26][CH2:25][CH2:24][CH2:23]2)[CH2:15][CH2:14]1>>[CH2:22]([NH:21][C@H:2]([C:1]([OH:12])=[O:11])[CH2:3][C:4]1[CH:5]=[CH:6][CH:7]=[CH:8][CH:9]=1)[CH2:27][CH2:26][CH2:25][CH2:24][CH2:23][CH2:1][CH2:2][CH2:3][CH3:4].[NH2:21][C:20]1[CH:13]=[CH:14][CH:15]=[CH:16][N:19]=1参加物
3
実験手順
The acylated phenylalanine anilide imprint molecule was synthesized in three steps. (1) N-α-t-BOC-L-phenylalanine was coupled with 2-aminopyridine using DCC to give N-α-t-BOC-L-phenylalaniine-2-aminopyridine. (2) The a-amine was then deprotected with TFA to give N-α-L-phenylalanine-2-aminopyridine. (3) To create a compound having the properties of a surfactant, the free amine was then acylated with decanoic acid using DCC to give N-α-decyl-L-phenylalanine-2-aminopyridine.
出典と根拠
- ORDレコード
- ord-4eddb75f7dab42a693198cb7ff2c3dcd
- 出典データセット
- uspto-grants-2003_12
- 特許番号
- US06660780B2
関連ノート
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