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HRID 432628作成日:2026年10月27日

2,3,5,6-Tetrafluorophenol → 3,4-Bis(4-methoxyphenyl)-6-(2,3,5,6-tetrafluorophenoxy)pyridazine

https://huagongshe.com/reaction/432628

反応式

関与物質

役割名称HCID仕込み量
反応物2,3,5,6-TetrafluorophenolHCID 69858—
反応物3,4-Bis(4-methoxyphenyl)-6-chloropyridazineHCID 12568084—
生成物3,4-Bis(4-methoxyphenyl)-6-(2,3,5,6-tetrafluorophenoxy)pyridazineHCID 10115219—

反応手順

In a similar manner as in Example 2, 3,4-bis(4-methoxyphenyl)-6-chloropyridazine (200 mg, 0.613 mmol) and 2,3,5,6-tetrafluorophenol were reacted as starting materials at 150° C. for 12 hours and post-treatment was then conducted, whereby the title compound was obtained as a colorless crystalline powder (105.7 mg, 37.8%). Melting point: 172.5-174.5° C. (hexane).

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US06664256B1
出典データセットuspto-grants-2003_12
ORD IDord-cf56bb63de004e00ad74b9a7c3eaaea2
出典メモuspto-grants-2003_12