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Ethyl 2-pyridylacetate → 1-Piperidineacetic acid, ethyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethyl 2-pyridylacetate | HCID 75960 | — |
| 反応物 | Ethyl 2-(piperidin-3-yl)acetate | HCID 2760464 | — |
| 生成物 | 1-Piperidineacetic acid, ethyl ester | HCID 643466 | — |
反応手順
The reaction was run in the same manner as ethyl 3-piperidinylacetate, starting with commercially available ethyl-2-pyridylacetate (4.00 g; 24.5 mmol). This gave ethyl 2-piperidinylacetate (2.41 g) as a light yellow oil without further purification. MS m/z (positive ion) 172 (MH+; 100).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06664271B1 |
| 出典データセット | uspto-grants-2003_12 |
| ORD ID | ord-885d55a01d27437bb29c8817847259b2 |
| 出典メモ | uspto-grants-2003_12 |